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PG Notes 2017 : Chemistry

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Banani Mukherjee
West Bengal State University (WBSU), Barasat, North 24 Parganas
B.SC CHEMISTRY
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SEMESTER-II Analytical Chemistry-II L-T-P: 3-1-0 Credit: 4 Unit-1: Spectroscopic techniques Theory, instrumentation and applications of X-rays (emission, absorption, diffraction and fluorescence methods), atomic absorption spectroscopy, atomic fluorescence spectrometry, atomic emission spectrometry, inductively coupled plasma-atomic absorption spectrometry. Unit-2: Electroanalytical methods Theory, instrumentation and applications of voltammetry, linear sweep voltammetry, anodic stripping voltammetry, cyclic voltammetry, amperometry, coulometry, electrogravimetry and polarography: electrochemical cell, reference and indicator electrodes, membrane electrodes, electrode-solution interface layer, electrolytic process, DME, Cottrell equation, Ilkovic equation, half wave potential and its significance, test of reversibility, current-voltage diagram. Unit-3: Thermal methods Theory, methodology and applications of thermogravimetric analysis (TGA), differential thermal analysis (DTA), and differential scanning calorimetry (DSC), thermal stability of covalent and non-covalent bonds, thermal degradation, single crystal phase transformation, thermochemiluminescence, thermometric titration, solid state reaction kinetics. Books recommended: 1. R. L. Pecsok, L. D. Shields, T. Cairns and L.C. Mc William, Modern Methods of Chemical nd Analysis, 2 Edition (1976), John Wiley, New York. th 2. G. D. Christian, Analytical Chemistry, 5 Edition (1994), John Wiley & Sons, New York. 3. D.A. Skoog, Principles of Instrumental Analysis, 5th Edition (1998), Saunders College of Publishing, Philadelphia, London. 4. D. A. Skoog, D.M. West, F.J. Holler, S.R. Crouch, Analytical Chemistry - An Introduction, th 7 Edition (2000), Saunders College Publishing, Philadelphia, London. nd 5. J. H. Kennedy, Analytical Chemistry: Principles, 2 Edition (1990), Saunders Holt, London. 6. A. J. Bard, Electroanalytical Chemistry 7. J. W. Robinson, Atomic absorption Spectrometry 8. D. A. Skoog, D.M. West, F.J. Holler, Fundamentals of Analytical Chemistry 9. H. H. Willard, L. L. Meritt, J. A. Dean and F. A. Settle, Instrumental Methods of Analysis 10. H.A. Strobel, Chemical Instrumentation: A Schematic Approach, 2nd Edition (1973), Addison Wesley, Reading, Mass. Inorganic Chemistry-II

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